The iron-catalyst compound, cas is 1271-42-7 name is Ferrocenecarboxylic acid, mainly used in chemical industry, its synthesis route is as follows.,1271-42-7
Chlorocarbonyl ferrocene 2b: The synthesis of chlorocarbonyl ferrocene 2b was adapted from a procedure of Cormode et al. {Dalton Trans. 2010, 39, 6532). After suspending ferrocenecarboxylic acid 2a (462 mg, 2.01 mmol) in dry CH2CI2 (23 mL), oxalyl chloride (1 100 mu, 13.64 mmol) in dry CH2CI2 (10 mL) was added dropwise to the reaction mixture whereby the orange suspension turned dark red. The reaction mixture was refluxed for 2 h and then stirred overnight at room temperature. The solvent was then removed under vacuum. The product 2 was not purified and used immediately for the next synthetic step.
With the rapid development of chemical substances, we look forward to future research findings about 1271-42-7
Reference£º
Patent; UNIVERSITAeT ZUeRICH; THE UNIVERSITY OF MELBOURNE; GASSER, Gilles; GASSER, Robin B.; HESS, Jeannine; JABBAR, Abdul; PATRA, Malay; WO2015/44395; (2015); A1;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion