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This work describes the preparation of nanocrystalline-graphite inlaid ring ultramicroelectrodes (UMEs) with inner diameters larger than 0.3 mum and thicknesses as low as a few nanometers. The geometric parameters of these UMEs were determined by a combination of optical microscopy and cyclic voltammetry data. These UMEs permit to establish mass-transport rates as large as those obtained on nanometer-sized hemispherical UMEs. They have very low electrochemical activity in acid and can function very well as catalyst supports for kinetic studies of fuel cell reactions such as the hydrogen oxidation reaction (hor). In order to demonstrate the outstanding utility of these electrodes, compact Pt films were electrodeposited on graphite ring UMEs and used to carry out a kinetic study of the hor in acid medium.
If you are interested in 1273-86-5, you can contact me at any time and look forward to more communication. The potential utility of systematic synthetic strategy will be applicable to efficient generations of chemical libraries of compounds to find ‘hit’ molecules. category: iron-catalyst
Reference：
Iron Catalysis in Organic Synthesis | Chemical Reviews,
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion