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A simple chromatography-free method for desymmetrizing ferrocene is described starting from the readily available dialdehyde. Oxidation of 1,1?-ferrocenedicarboxaldehyde in a water/acetonitrile mixture with KMnO4 produced 1?-formyl-ferrocenecarboxylic acid. The same reaction carried out in a water/acetone mixture produced 1?-[(E)-3-oxo- but-1-enyl]-ferrocenecarboxylic acid.
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Reference：
Iron Catalysis in Organic Synthesis | Chemical Reviews,
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion